Ionic crystals

Scanning force microscopy examples: Ionic crystals

Ionic crystals can easily be cleaved and are - like e.g. also graphite - frequently used to check the noise level of the instrument and the z calibration of the scanner. On the small scale, steps and screw dislocations are visible.
KBr (lattice constant 330pm)
Derivative of the topographic signal, image size 13 µm. Instrument: Digital Instruments Nanoscope IIIa Multimode, in Tapping Mode.
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image
On a larger scale, the circular hills are arranged in a well-ordered structure.ee
Image size 50 µm; topographic image (z scale 40 nm)
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full size image

Image size 50 µm; topographic image (z scale 40 nm) and derivative of topography.
Instrument: Park Scientific Instruments Autoprobe CP, in Intermittent Contact Mode.
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the full size image
Images with atomic resolution are possible in ultrahigh-vacuum, obtained with a home-built instrument based on a qPlus force sensor (Markus Herz 2002, unpublished). Topographic image of KCl (lattice constant 315pm), image size 1.9nm, height variation approx. 50pm.


© 2012
Experimental Physics VI
Institute of Physics
University of Augsburg
last updated: 04/30/2012, 09:21
http://www.physik.uni-augsburg.de/exp6/research/sxm/ionic/ionic_e.shtml